A STUDY ON HYDROTHERMAL SYNTHESIS OF METAL–ORGANIC FRAMEWORK MIL-101

Võ Thị Thanh Châu, Hoàng Văn Đức

DOI: http://dx.doi.org/10.26459/hueuni-jns.v126i1C.4417

Abstract


In the present paper, a synthesis of MIL-101 by hydrothermal process was demonstrated. The obtained samples were characterized by powder X-ray diffraction (PXRD), transmission electron microscope (TEM), nitrogen adsorption/desorption isotherms at 77K, X-ray photoelectron spectroscopy (XPS). The results showed that MIL-101 synthesized by optimal conditions exhibited high crystallinity and surface area. The obtained MIL-101 possesses high stability in water and several organic solvents.

Keywords: MIL-101, hydrothermal synthesis, metal organic framework-101. 


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